NDLI: Phase transitions in A$_{4}$Li(HSO$_{4}$)$_{3}$(SO$_{4}$); A = Rb, K: Single crystal X-ray diffraction studies

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Phase transitions in A$_{4}$Li(HSO$_{4}$)$_{3}$(SO$_{4}$); A = Rb, K: Single crystal X-ray diffraction studies

Content Provider	SpringerLink
Author	Nalini, G. Row, T. N. Guru
Copyright Year	2003
Abstract	The crystal structure of ferroelastic Rb$_{4}$Li(HSO$_{4}$)$_{3}$(SO$_{4}$) has been determined at two temperatures, which indicates a structural phase transition, tetragonal P4$_{3}$ witha = 7.629(1) Å,c = 29.497(2) Å at 293 K and monoclinic P2$_{1}$ witha = 7.583(3) Å,b = 29.230(19) Å,c = 7.536(5) Å,β = 90.14(1)° at 90 K. The crystal structure of K$_{4}$Li(HSO$_{4}$)$_{3}$(SO$_{4}$)$_{4}$ has also been determined at two temperatures, tetragonalP4$_{1}$ witha = 7.405(1) Å,c = 28.712(6) Å at 293 K and tetragonalP4$_{1}$ witha = 7.371(5) Å,c = 28.522(5) Å at 100 K. The overall coordination features in both the structures have been analysed in terms of bond valence sum calculations.
Starting Page	473
Ending Page	490
Page Count	18
File Format	PDF
ISSN	02534134
Journal	Journal of Chemical Sciences
Volume Number	115
Issue Number	5-6
e-ISSN	09737103
Language	English
Publisher	Springer India
Publisher Date	2003-01-01
Publisher Institution	Indian Academy of Sciences
Publisher Place	New Delhi
Access Restriction	Subscribed
Subject Keyword	Phase transition ferroelastic cryo-crystallography crystal structure Chemistry/Food Science
Content Type	Text
Resource Type	Article

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