NDLI: Synthesis and Characterization of Some Triphenyltin(IV) Complexes from Sterically Crowded [((E)-1-{2-Hydroxy-5-[(E)-2-(aryl)-1-diazenyl]phenyl}methylidene)amino]acetate Ligands and Crystal Structure Analysis of a Tetrameric Triphenyltin(IV) Compound

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Synthesis and Characterization of Some Triphenyltin(IV) Complexes from Sterically Crowded [((E)-1-{2-Hydroxy-5-[(E)-2-(aryl)-1-diazenyl]phenyl}methylidene)amino]acetate Ligands and Crystal Structure Analysis of a Tetrameric Triphenyltin(IV) Compound

Content Provider	SpringerLink
Author	Basu Baul, Tushar S. Das, Pradip Eng, George Linden, Anthony
Copyright Year	2010
Abstract	Four new triphenyltin(IV) complexes containing [((E)-1-{2-hydroxy-5-[(E)-2-(aryl)-1-diazenyl]phenyl}methylidene)amino]acetate ligands (L) have been synthesized with formulations of Ph$_{3}$SnLH. They have been studied by multinuclear ($^{1}$H, $^{13}$C, $^{119}$Sn) NMR, $^{119}$Sn Mössbauer and IR spectroscopy. A full characterization of one complex, Ph$_{3}$SnL$^{1}$H (1), was accomplished by single crystal X-ray crystallography, which revealed the compound to be a macrocyclic tetramer. In the tetramer, the five coordinate tin atoms have distorted trigonal bipyramidal geometries with the three phenyl groups occupying equatorial positions, while an oxygen atom of the carboxylate group of one L ligand and the oxide O-atom (formerly the hydroxy group) of a second L ligand in an apical positions. The carboxylate ligands bridge adjacent tin atoms and coordinate in the zwitterionic form with the phenolic proton moved to the nearby nitrogen atom. $^{119}$Sn NMR results indicate that the tetrameric structures of the complexes in the solid state, in which the tin atoms are five-coordinated, dissociate in solution to yield four coordinate monomeric species.
Starting Page	134
Ending Page	141
Page Count	8
File Format	PDF
ISSN	15741443
Journal	Journal of Inorganic and Organometallic Polymers and Materials
Volume Number	20
Issue Number	1
e-ISSN	15741451
Language	English
Publisher	Springer US
Publisher Date	2010-01-20
Publisher Place	Boston
Access Restriction	Subscribed
Subject Keyword	Triphenyltin Carboxylates [((E)-1-{2-hydroxy-5-[(E)-2-(aryl)-1-diazenyl]phenyl}methylidene)amino]acetate Crystal structure Polymer Sciences Organic Chemistry Inorganic Chemistry
Content Type	Text
Resource Type	Article
Subject	Materials Chemistry Polymers and Plastics

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Synthesis and Characterization of Some Triphenyltin(IV) Complexes from Sterically Crowded [((E)-1-{2-Hydroxy-5-[(E)-2-(aryl)-1-diazenyl]phenyl}methylidene)amino]acetate Ligands and Crystal Structure Analysis of a Tetrameric Triphenyltin(IV) Compound

Synthesis, Spectroscopic Characterization and Structures of Tributyltin(IV) 4-[((E)-1-{2-hydroxy-5-[(E)-2-(aryl)-1-diazenyl]phenyl}methylidene)amino]benzoates. Toxicity Studies on the Second Larval Instar of the Anopheles stephensi Mosquito Larvae

Synthesis , characterization and crystal structures of polymeric and dimeric triphenyltin ( IV ) complexes of 4-[ ( ( E )-1-{ 2-hydroxy-5-[ ( E )-2-( 2-carboxyphenyl )-1-diazenyl ] phenyl } methylidene ) amino ] aryls

119Sn Mössbauer, NMR (1H, 13C and 119Sn) and infrared study of tetracoordinated tin(IV) complexes with 4-[((E)-1-{2-hydroxy-5-[(E)-2-(aryl)-1-diazenyl]phenyl}methylidene)amino]benzoates

Synthesis and Characterization of Archetypal Ladder-Like Dibutyloxotin Cluster Derived from Sterically Encumbered 4-[(E)-2-(4-hydroxy-5-methylphenyl)-1-diazenyl]benzoate

Crystal structure of 5-[(E)-2-phenyl-1-diazenyl]-(2-hydroxy-benzenecarboxylato-O,O′)titanocene—dichloromethane (1:0.5), (C6H7)2Ti(C13H8N2O3) · 0.5CH2Cl2

Synthesis of methyl 3-acyl-6-amino-5-cyano-4-phenyl-4H-pyran-2-carboxylates and their rearrangement into 2-hydroxy-4-[hydroxy(R)methylidene]-3-oxo-5-phenylcyclopent-1-ene-1-carbonitriles

(E)-1-{2-Hydroxy-5-[(4-methylphenyl)diazenyl]phenyl}ethanone

Crystal structure of (E)-2-({4-hydroxy-5-methoxy-3-[(4-methyl-1-piperazinyl)methyl]phenyl} methylidene)-1-indanone, C23H26N2O3

Synthesis and Characterization of Some Triphenyltin(IV) Complexes from Sterically Crowded [((E)-1-{2-Hydroxy-5-[(E)-2-(aryl)-1-diazenyl]phenyl}methylidene)amino]acetate Ligands and Crystal Structure Analysis of a Tetrameric Triphenyltin(IV) Compound

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