Thumbnail
Access Restriction
Open

Author Habibi, Mohammad Hossein ♦ Barati, Kazem ♦ Zendehdel, Mahmoud ♦ Harrington, Ross W. ♦ Clegg, William
Source J-STAGE
Content type Text
Publisher The Japan Society for Analytical Chemistry
Language English
Abstract The structure of N,N′-bis(3-nitroobenzylidene)butane-1,4-diamine was determine by X-ray crystallography. The symmetry operation (-x + 2, -y + 1, -z) generates the whole molecule. The compound crystallizes in a monoclinic system and was characterized thus: $P2_{1}/c,$ a = 4.981(5), b = 11.205(7), c = 15.134(12)Å, β = 92.28(4)°, Z = 2, V = $843.9(12)Å^{3}.$ The crystal structure was solved by direct methods and refined by full-matrix least-squares on $F^{2}$ to final values of R = 0.0624 and wR = 0.1329.
Learning Resource Type Article
Publisher Date 2007-01-01
e-ISSN 13482238
Journal Analytical Sciences: X-ray Structure Analysis Online(analscix)
Volume Number 23


Open content in new tab

   Open content in new tab