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Author Fauth, M. I. ♦ McNerney, C. F.
Sponsorship USDOE
Source United States Department of Energy Office of Scientific and Technical Information
Content type Text
Language English
Subject Keyword CHEMISTRY ♦ ACETIC ACID ♦ AIR ♦ BORON COMPOUNDS ♦ BORON HYDRIDES ♦ HEATING ♦ HELIUM ♦ IODATES ♦ IODINE ♦ MEASURED VALUES ♦ OXIDATION ♦ POTASSIUM COMPOUNDS ♦ QUANTITATIVE ANALYSIS ♦ RECOVERY ♦ SOLVENTS ♦ STABILITY ♦ TEMPERATURE
Abstract ABS>A method for the quantitative determination of decaborane consists of oxidation with pctassium icdate, reaction of excess iodate with potassium iodide, and titration of the liberated iodine with scdium thiosulfate. Acetic acid was found to be the most satisfactory solvent for the decaborane. Recoveries on the order of 98% have been obtained. Differential thermal analysis curves are presented for decaborane heated in air and in helium for the temperature range 20 deg to 150 deg C. (auth)
ISSN 00032700
Educational Use Research
Learning Resource Type Article
Publisher Date 1960-01-01
Publisher Department U.S. Naval Propellant Plant, Indian Head, Md.
Journal Analytical Chemistry
Volume Number 32
Organization U.S. Naval Propellant Plant, Indian Head, Md.


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